QUANTIFICATION OF ETHANOL AND ACIDITY IN FERMENTED FRUIT VINEGAR FOR HALAL CERTIFICATION ANALYSIS

Authors

  • Adi Permadi Universitas Ahmad Dahlan Yogyakarta Author
  • Siswanto Masruri Universitas Ahmad Dahlan Yogyakarta Author
  • Mhd Lailan Arqam Universitas Ahmad Dahlan Yogyakarta Author
  • Arina Aprillia Syahputri Universitas Ahmad Dahlan Yogyakarta Author

DOI:

https://doi.org/10.54783/g3ytez88

Keywords:

Ethanol Content, Fermented Vinegar, Halal Food; MUI Fatwa, Total Acidity

Abstract

Fermented vinegar products are increasingly gaining popularity as natural health supplements. However, the presence of ethanol as a by-product of the fermentation process places vinegar in a critical position in determining its halal status, particularly after the issuance of MUI Fatwa No. 10 of 2018, which stipulates that halal beverages must contain less than 0.5% ethanol (v/v). This study aims to determine the ethanol content and total acidity of various fruit vinegar products available on the market. Eight samples were analyzed using distillation UV–Vis spectrophotometry to quantify ethanol levels and acid–base titration to determine total acidity. The results demonstrated that all samples including apple, pineapple, pear, and orange vinegar contained non-detectable ethanol levels (0.00%) and total acidity values ranging from 1.38% to 7.69%. These findings indicate that the two-stage fermentation process alcoholic fermentation followed by acetic fermentation occurred optimally, resulting in complete oxidation of ethanol into acetic acid during product formation. Consequently, all samples met the halal criteria specified in Fatwa MUI 2018, as none exceeded the permissible ethanol threshold and none originated from khamr. This study confirms that fermented fruit vinegar marketed in the community is safe and halal for consumption, while also emphasizing the importance of laboratory-based halal literacy as a scientific foundation for strengthening public awareness of food safety and religious compliance.

References

1. An-Nawawi, Y. (n.d.). Sharḥ Ṣaḥīḥ Muslim (Vol. 13). Beirut, Lebanon: Dār al-Kutub al-ʿIlmiyyah.

2. Abu Dawud, S. (2008). Sunan Abi Dawud (Hadith No. 3681). Riyadh, Saudi Arabia: Darussalam Publications.

3. Abu Dawud, S. (2009). Sunan Abi Dawud (Hadith No. 3675). Riyadh, Saudi Arabia: Darussalam Publications.

4. Boasiako, T. A., Boateng, I. D., Ekumah, J., Adwoa, N., Johnson, N., Appiagyei, J., Murtaza, M. S., Mubeen, B., & Ma, Y. (2024). Advancing Sustainable Innovations in Mulberry Vinegar Production : A Critical Review on Non-Thermal Pre-Processing Technologies.

5. Khalifa, S. A. M., El-Shabasy, R. M., Tahir, H. E., Abo-Atya, D. M., Saeed, A., Abolibda, T. Z., Guo, Z., Zou, X., Zhang, D., Du, M., Kai, G., Buccato, D. G., Daglia, M., Zhao, C., & El-Seedi, H. R. (2024). Vinegar – a beneficial food additive: Production, safety, possibilities, and applications from ancient to modern times. Food & Function, 15(20), 10262–10282. https://doi.org/10.1039/d4fo02377c

6. Di Vincenzo, A., Tana, C., El Hadi, H., Pagano, C., Vettor, R., & Rossato, M. (2019). Antioxidant, anti-inflammatory, and metabolic properties of tocopherols and tocotrienols: Clinical implications for vitamin E supplementation in diabetic kidney disease. International Journal of Molecular Sciences, 20(20). https://doi.org/10.3390/ijms20205101

7. Haider, N. (2013). Contesting Intoxication : Early Juristic Debates over the Lawfulness of Alcoholic Beverages *. 48–89. https://doi.org/10.1163/15685195-0002A0002

8. Harahap, I., Shukri, A.S.M., Jamaludin, M.A., Nawawi, N., Alias, R. and Zaharim, A. (2020). The application of taḥawwul ( transformation ) process for determination of. Food Research, 4(June), 896–905. http://www.myfoodresearch.com

9. Ibn Muflih, S. (n.d.). Al-Ādāb al-Sharʿiyyah (Vol. 3). Beirut, Lebanon: Dār al-Kutub al-ʿIlmiyyah

10. Jamilah, S., Sukri, M., Mat, M., Shamsuddin, J., Anuar, M., Rohman, A., Sutoyo, S., & Ahmad, N. (2022). Sains Humanika A Guideline of Determination Haram Status of Intentionally Adding Animal Plasma in Surimi Products. 3, 29–47.

11. Luzón-Quintana, L. M., Castro, R., & Durán-Guerrero, E. (2021). Biotechnological processes in fruit vinegar production. Foods, 10(5), 945. https://doi.org/10.3390/foods10050945

12. Mat Isham, N. K., Mokhtar, N., Fazry, S., & Lim, S. J. (2018). The development of an alternative fermentation model system for vinegar production. LWT – Food Science and Technology. https://doi.org/10.1016/j.lwt.2018.10.065

13. Mukherjee, A., Gómez-sala, B., Connor, E. M. O., & Kenny, J. G. (2022). Global Regulatory Frameworks for Fermented Foods : A Review. 9(May), 0–20. https://doi.org/10.3389/fnut.2022.902642

14. Muslim, (2007). Ṣaḥīḥ Muslim (Hadith No. 2003). Riyadh, Saudi Arabia: Darussalam Publications.

15. Nandala, I. M., Azrak, T., & Economic, I. (2024). Halal Certification : Legal And Ethical Consideration IN. 9(2), 43–60.

16. Radhiah, S., & Nazirah, S. (2018). Reviving The Authenticity Of Prophetic ( Sunnah ) Drinks In Beverage Industry In Malaysia : A Review. 505–520.

17. Sumiyani, R., Budiono, R., Khamila, H. M., Pramesti, T. A., Departement, P., Surabaya, U., Rungkut, K., & Program, F. E. (2024). Determination of ethanol and acetic acid content in local brands of apple vinegar : gas chromatography test for halal requirements. 137–146. https://doi.org/10.20473/jhpr.vol.7-issue.2.137-146

18. Tamizi, S. M., Suliaman, I., & Ibrahim, H. (n.d.). The prophetic tradition and nutrition : issues of mixing raisins and dates. https://doi.org/10.15364/ris14-0102-06

19. Vojir, F., Schübl, E., & Elmadfa, I. (2012). The Origins of a Global Standard for Food Quality and Safety : Codex Alimentarius Austriacus and FAO / WHO Codex Alimentarius. 82(3), 223–227. https://doi.org/10.1024/0300

20. Wijayant, R., & Kaukab, M. E. (2019). Istihalah issue of halal food, medicine, and cosmetics. Journal of Islamic, Social, Economics and Development (JISEd), 4(19), 203–213.Winarno. (2018). Status hukum khamar dalam persfektif fiqh. Asy Syar’iyyah: Jurnal Ilmu Syari’ah Dan Perbankan Islam, 3(1), 1–25. https://jurnal.lp2msasbabel.ac.id

21. Xia, T., Zhang, B., Duan, W., Zhang, J., & Wang, M. (2020). Nutrients and bioactive components from vinegar : A fermented and functional food. Journal of Functional Foods, 64(August 2019), 103681. https://doi.org/10.1016/j.jff.2019.103681

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Published

17-03-2026

How to Cite

QUANTIFICATION OF ETHANOL AND ACIDITY IN FERMENTED FRUIT VINEGAR FOR HALAL CERTIFICATION ANALYSIS. (2026). Iqtishaduna : International Conference Proceeding, 2, 220-228. https://doi.org/10.54783/g3ytez88

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